Microwave-assisted synthesis of zinc 5-(4-carboxyphenyl)-10,15,20-triphenylporphyrin and zinc 5-(4-carboxyphenyl)-10,15,20-triphenylchlorin - Université de Lorraine Accéder directement au contenu
Article Dans Une Revue Journal of Porphyrins and Phthalocyanines Année : 2015

Microwave-assisted synthesis of zinc 5-(4-carboxyphenyl)-10,15,20-triphenylporphyrin and zinc 5-(4-carboxyphenyl)-10,15,20-triphenylchlorin

Résumé

The microwave-assisted synthesis of zinc 5-(4-carboxyphenyl)-10,15,20-triphenylporphyrin and zinc 5-(4-carboxyphenyl)-10,15,20-triphenylchlrorin are described and compared to classic conditions of synthesis in terms of time of reaction and yields obtained. The new experimental protocols are easy to implement required small amounts of reagents and solvents and lead to short reaction times. All compounds have been characterized by H-1 NMR, MS and spectroscopic techniques.

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Chimie
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Dates et versions

hal-01267219 , version 1 (04-02-2016)

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Rima Chouikrat, Aymeric Champion, Régis Vanderesse, Céline Frochot, Albert Moussaron. Microwave-assisted synthesis of zinc 5-(4-carboxyphenyl)-10,15,20-triphenylporphyrin and zinc 5-(4-carboxyphenyl)-10,15,20-triphenylchlorin. Journal of Porphyrins and Phthalocyanines, 2015, 19 (4), pp.595-600. ⟨10.1142/S1088424614500953⟩. ⟨hal-01267219⟩
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